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🍳Separation Processes

Key Concepts of Evaporation Equipment

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Why This Matters

Evaporation is one of the most energy-intensive unit operations you'll encounter in separation processes, and exam questions love to test whether you understand why engineers choose one evaporator type over another. You're not just being asked to identify equipment—you're being tested on the underlying principles of heat transfer efficiency, energy recovery, fluid dynamics, and material sensitivity. Every evaporator design represents a trade-off between these factors.

When you study this topic, think about what problem each design solves. Is it maximizing energy efficiency? Handling viscous or fouling fluids? Protecting heat-sensitive products? Don't just memorize the names—know what concept each evaporator illustrates and when you'd recommend it over alternatives.


Energy Recovery Systems

The biggest operating cost in evaporation is steam. These designs focus on reusing thermal energy rather than discarding it, dramatically reducing utility costs in large-scale operations.

Multiple-Effect Evaporators

  • Vapor from one effect heats the next—each subsequent stage operates at lower pressure and temperature, allowing heat reuse without additional steam input
  • Energy efficiency scales with number of effects—a triple-effect system uses roughly one-third the steam of a single-effect unit for the same evaporation capacity
  • Industry workhorse for large-scale concentration—dominant in sugar refining, pulp and paper, and chemical manufacturing where throughput justifies capital cost

Mechanical Vapor Recompression (MVR) Evaporators

  • Compressor raises vapor pressure and temperature—the evaporator's own vapor becomes the heating medium after mechanical compression, creating a nearly closed energy loop
  • Highest energy efficiency available—can reduce steam consumption by 90%+ compared to single-effect systems, though electrical costs for compression must be considered
  • Operates at lower temperatures—ideal for heat-sensitive materials like fruit concentrates and pharmaceutical intermediates

Thermal Vapor Recompression (TVR) Evaporators

  • Steam jet ejector compresses vapor—uses high-pressure motive steam to entrain and compress low-pressure vapor for reuse
  • Lower capital cost than MVR—no moving parts in the ejector, making it simpler to maintain and install
  • Best when steam is cheap and abundant—common in facilities with existing boiler infrastructure or waste heat availability

Compare: MVR vs. TVR—both recover vapor energy, but MVR uses electricity while TVR uses steam. Choose MVR when electricity is cheaper than steam or when you need maximum efficiency; choose TVR when you have excess low-cost steam and want lower capital investment.


Film-Based Heat Transfer

These designs maximize the heat transfer coefficient by creating thin liquid films with high surface-area-to-volume ratios. The key principle: thinner films mean faster heat transfer and shorter residence times.

Falling Film Evaporators

  • Liquid flows as thin film down vertical tubes—gravity drives flow while steam heats the outer tube surface, achieving heat transfer coefficients of 10003000W/m2K1000–3000 \, \text{W/m}^2\text{K}
  • Minimal residence time (seconds)—critical for heat-sensitive products like fruit juices, milk, and enzymes that degrade at elevated temperatures
  • Requires uniform feed distribution—poor distribution causes dry spots and fouling; typically needs minimum flow rates to maintain film integrity

Rising Film Evaporators

  • Vapor bubbles lift liquid upward—boiling at the tube bottom creates vapor that carries liquid film up the tube walls, enabling self-pumping action
  • Handles moderate viscosity fluids—the vapor-lift mechanism works well with thicker feeds that would struggle in falling film designs
  • Higher temperature driving force—operates with greater ΔT\Delta T than falling film, enabling rapid evaporation for less temperature-sensitive materials

Agitated Thin-Film Evaporators

  • Mechanical blades spread liquid into thin film—rotating wiper blades continuously renew the heat transfer surface, preventing buildup and ensuring uniform thickness
  • Shortest residence time (seconds)—combined with precise temperature control, ideal for thermally unstable compounds and high-value specialty chemicals
  • Handles extreme viscosity—can process materials up to 100,000cP100,000 \, \text{cP} that would be impossible in gravity-driven film evaporators

Compare: Falling film vs. agitated thin-film—both minimize residence time for heat-sensitive materials, but falling film is simpler and cheaper for low-viscosity feeds, while agitated thin-film handles viscous, fouling, or extremely sensitive materials at higher capital cost.


Circulation and Fouling Control

When fluids are viscous, contain suspended solids, or tend to deposit scale, forced movement prevents the buildup that kills heat transfer efficiency.

Forced Circulation Evaporators

  • External pump maintains high velocity—liquid velocities of 25m/s2–5 \, \text{m/s} scour heat transfer surfaces, preventing crystallization and fouling
  • Handles high solids and scaling solutions—the go-to design for salt crystallization, caustic concentration, and wastewater with suspended particles
  • Heat exchanger separate from flash chamber—liquid is heated under pressure in tubes, then flashes in a separate vessel, protecting the heat exchanger from boiling-induced deposits

Single-Effect Evaporators

  • Simplest configuration—feed enters, steam heats, concentrate exits; all evaporation occurs in one stage with no energy recovery
  • Lowest capital cost, highest operating cost—appropriate only for small-scale operations, batch processes, or situations where steam is essentially free
  • Baseline for understanding efficiency gains—multiple-effect and vapor recompression systems are measured against single-effect steam economy (1kg evaporation/kg steam\approx 1 \, \text{kg evaporation/kg steam})

Compare: Forced circulation vs. falling film—forced circulation handles fouling and viscous feeds but requires pump energy and has longer residence times; falling film is more efficient for clean, low-viscosity feeds but cannot tolerate fouling conditions.


Specialized Separation Mechanisms

These designs exploit specific physical phenomena—rapid pressure drops or compact geometry—to achieve separation goals beyond simple concentration.

Flash Evaporators

  • Instantaneous vaporization via pressure drop—superheated liquid enters a low-pressure chamber and partially vaporizes without external heating in that stage
  • Separates volatile from non-volatile components—useful for stripping dissolved gases, removing light solvents, or multi-stage desalination
  • Often combined with other evaporator types—flash chambers frequently follow heat exchangers in multi-stage thermal desalination (MSF) systems

Plate Evaporators

  • Corrugated plates create turbulent flow—high shear rates in narrow channels enhance heat transfer while keeping equipment footprint small
  • Easy disassembly for cleaning—plates can be separated for inspection and CIP (clean-in-place), critical for food and pharmaceutical sanitation requirements
  • Limited to low-viscosity fluids—narrow channels restrict flow of thick materials; best for milk, juices, and light chemical solutions

Compare: Flash evaporators vs. plate evaporators—flash evaporators exploit pressure-driven phase change for volatile separation, while plate evaporators maximize heat transfer surface area in compact space. Flash is about what vaporizes; plate is about how efficiently you transfer heat.


Quick Reference Table

ConceptBest Examples
Energy recovery via vapor reuseMultiple-effect, MVR, TVR
Heat-sensitive material handlingFalling film, MVR, agitated thin-film
High viscosity processingForced circulation, rising film, agitated thin-film
Fouling/scaling resistanceForced circulation, agitated thin-film
Compact design/easy cleaningPlate evaporators
Volatile component separationFlash evaporators
Low capital cost (small scale)Single-effect
Maximum energy efficiencyMVR, multiple-effect (many stages)

Self-Check Questions

  1. Which two evaporator types both recover vapor energy but differ in their energy input—and when would you choose each?

  2. A pharmaceutical company needs to concentrate a heat-sensitive enzyme solution with moderate viscosity. Which evaporator type would you recommend, and what principle makes it suitable?

  3. Compare falling film and forced circulation evaporators: what feed characteristics would push you toward each design?

  4. If an FRQ asks you to design an evaporation system for a crystallizing salt solution that tends to foul heat transfer surfaces, which evaporator type is your best answer and why?

  5. Rank single-effect, triple-effect, and MVR evaporators by steam economy—then explain the trade-off that might still make single-effect the right choice in certain situations.